N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

Base Information

• Chemical Name: N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal
• CAS No.: 76992-52-4
• Molecular Formula: C₃₇H₄₅NO₇
• Molecular Weight: 615.767

Synonyms:N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

Chemical Property of N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

Chemical Property:

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Technology Process of N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

There total 2 articles about N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.8%

[1-(3,5-Bis-benzyloxy-phenyl)-meth-(Z)-ylidene]-(2,2-diethoxy-ethyl)-amine (60095-69-4) + 5-(chloromethyl)-1,2,3-trimethoxybenzene (3840-30-0) → 1,2-Bis-(3,5-bis-benzyloxy-phenyl)-N,N'-bis-(2,2-diethoxy-ethyl)-ethane-1,2-diamine (84423-17-6) + N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal (76992-52-4)

Guidance literature:

With magnesium; In tetrahydrofuran; for 1h; Yields of byproduct given; Heating;

DOI:10.1248/cpb.30.3197

Reference yield:

[1-(3,5-Bis-benzyloxy-phenyl)-meth-(Z)-ylidene]-(2,2-diethoxy-ethyl)-amine (60095-69-4) + 5-(chloromethyl)-1,2,3-trimethoxybenzene (3840-30-0) → brittonin A (33284-74-1) + N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal (76992-52-4)

Guidance literature:

With magnesium; In tetrahydrofuran; Yield given; 1.) 3 deg C, 40 min, 2.) 0 to room temp. overnight;

DOI:10.1248/cpb.30.3197

Reference yield: 84.0%

benzyl chloroformate (501-53-1,94274-21-2) + N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal (76992-52-4) → N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal (79539-44-9)

Guidance literature:

With sodium hydrogencarbonate; In chloroform; water; 2 deg C, 0.5 h, room temp. 1 h;

DOI:10.1248/cpb.30.3197

upstream raw materials:

[1-(3,5-Bis-benzyloxy-phenyl)-meth-(Z)-ylidene]-(2,2-diethoxy-ethyl)-amine

5-(chloromethyl)-1,2,3-trimethoxybenzene

Downstream raw materials:

N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

(+/-)-TA-073

N-benzyloxycarbonyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2-dihydroisoquinoline

C₄₁H₃₉NO₇

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