Au2Cl2{μ-Ph2P(CH2)6PPh2}

Base Information

Chemical Name:Au2Cl2{μ-Ph2P(CH2)6PPh2}
CAS No.:64659-16-1
Molecular Formula:C₃₀H₃₂Au₂Cl₂P₂
Molecular Weight:919.371
Hs Code.:

Synonyms:Au2Cl2{μ-Ph2P(CH2)6PPh2}

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Chemical Property of Au2Cl2{μ-Ph2P(CH2)6PPh2}

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Technology Process of Au2Cl2{μ-Ph2P(CH2)6PPh2}

There total 4 articles about Au2Cl2{μ-Ph2P(CH2)6PPh2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 29892-37-3
chloro(dimethylsulfide) gold(I)

: 19845-69-3
1,6-bis(diphenylphosphino)hexane

: 64659-16-1
Au2Cl2{μ-Ph2P(CH2)6PPh2}

Guidance literature:: In acetone; addn. of soln. of ((C6H5)2P)2(CH2)6 (1 equiv.) in acetone to suspn. of (AuCl(SMe)2) (2 equiv.) in acetone; stirring for 2 h; pptn., filtration, washing with acetone, diethyl ether and pentane, drying under vac.;
DOI:10.1039/b005251p

Reference yield:

: 69462-32-4
cloro(thiodiethanol)gold(I)

: 19845-69-3
1,6-bis(diphenylphosphino)hexane

: 64659-16-1
Au2Cl2{μ-Ph2P(CH2)6PPh2}

Guidance literature:: In methanol; dichloromethane; N2, stoich., a soln. of gold compd. (methanol) added to a soln. of phosphane (CH2Cl2), stirred for 24 h; solvent removed (vac.), water added, ppt. filtered, washed (water, diethyl ether), dried (vac.);
DOI:10.1002/ejic.200300774