4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile

Base Information

Chemical Name:4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile
CAS No.:1585273-78-4
Molecular Formula:C₂₁H₁₅N₅O₃
Molecular Weight:385.382
Hs Code.:

Synonyms:4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile

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Chemical Property of 4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile

Chemical Property:

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Technology Process of 4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile

There total 7 articles about 4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24484-96-6
2-amino-4-chloro-5-nitropyridine

: 1585273-78-4
4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / Inert atmosphere; Reflux

With palladium diacetate; potassium carbonate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.02.047

Reference yield:

: 623-00-7
4-bromobenzenecarbonitrile

: 1585274-88-9
C₁₄H₁₂N₄O₃

: 1585273-78-4
4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile

Guidance literature:: With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2014.02.047

Reference yield:

: 24484-93-3
4-Chloro-pyridine-2-carboxylic acid methyl ester

: 1585273-78-4
4-(2-(4-cyanophenylamino)-5-nitropyridin-4-yloxy)-3,5-dimethylbenzonitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: water / 0.25 h

1.2: 1 h / 20 °C

2.1: sodium hydroxide; bromine / water / 0.58 h / 0 - 5 °C

3.1: sulfuric acid; nitric acid / 0 - 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

5.1: palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / Inert atmosphere; Reflux

With sulfuric acid; bromine; nitric acid; palladium diacetate; potassium carbonate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.02.047