(2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid

Base Information

Chemical Name:(2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid
CAS No.:577978-91-7
Molecular Formula:C₃₆H₃₁NO₃
Molecular Weight:525.647
Hs Code.:

Synonyms:(2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid

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Chemical Property of (2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid

There total 5 articles about (2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 577978-90-6
(3R,4R)-3-O-benzyl-5-phenyl-4-[(9-phenyl-9-fluorenyl)-amino]-penten-3-ol

: 577978-91-7
(2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid

Guidance literature:: (3R,4R)-3-O-benzyl-5-phenyl-4-[(9-phenyl-9-fluorenyl)-amino]-penten-3-ol; With ozone; In methanol; at -78 ℃;

With dihydrogen peroxide; In methanol; at 20 ℃;

Reference yield: 87.0%

: 606124-56-5
((1R,2R)-1-Benzyl-2-benzyloxy-but-3-ynyl)-(9-phenyl-9H-fluoren-9-yl)-amine

: 577978-91-7
(2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid

Guidance literature:: With potassium permanganate; water; acetic acid; In pentane;
DOI:10.1016/S0040-4039(03)01394-7

Reference yield:

: 100-39-0
benzyl bromide

: 577978-91-7
(2S,3R)-2-O-benzyl-4-phenyl-3-[(9-phenyl-9-fluorenyl)-amino]-phenylbutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / NaH; Bu₄NI / tetrahydrofuran / 0 °C

2: 87 percent / KMnO₄; acetic acid; water / pentane

With potassium permanganate; water; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; In tetrahydrofuran; pentane;
DOI:10.1016/S0040-4039(03)01394-7