PChd-L-Leu-Gly-NH₂

Base Information

Chemical Name:PChd-L-Leu-Gly-NH₂
CAS No.:74763-81-8
Molecular Formula:C₂₈H₄₁N₃O₃
Molecular Weight:467.652
Hs Code.:

Synonyms:PChd-L-Leu-Gly-NH₂

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Chemical Property of PChd-L-Leu-Gly-NH₂

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Technology Process of PChd-L-Leu-Gly-NH₂

There total 15 articles about PChd-L-Leu-Gly-NH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 74763-78-3
PChd-L-Leu-OH

: 598-41-4
H-Gly-NH₂

: 74763-81-8
PChd-L-Leu-Gly-NH₂

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide;

Reference yield:

: 2668-47-5
2,6-di(t-butyl)-4-phenylphenol

: 74763-81-8
PChd-L-Leu-Gly-NH₂

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / 2,6-dimethylpyridine; tetraethylammonium tetrafluoroborate / CH₂Cl₂ / 8 h / anodic oxidation

2: 60 percent / 1 N NaOH / methanol / 4 h

3: 85 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 1.) 1 h, 0 deg C; 2.) 12 h at room temp.

With 2,6-dimethylpyridine; sodium hydroxide; N,N,N,N-tetraethylammonium tetrafluoroborate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1002/jlac.198219820608

Reference yield:

: 82636-91-7
PChd-L-Leu-Ala-OMe

: 74763-81-8
PChd-L-Leu-Gly-NH₂

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 1 N HCl, H₂ / Pd/10percent on charcoal / methanol / 4 h

2: 89 percent / 2,6-dimethylpyridine; tetraethylammonium tetrafluoroborate / CH₂Cl₂ / 8 h / anodic oxidation

3: 60 percent / 1 N NaOH / methanol / 4 h

4: 85 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 1.) 1 h, 0 deg C; 2.) 12 h at room temp.

With 2,6-dimethylpyridine; hydrogenchloride; sodium hydroxide; hydrogen; N,N,N,N-tetraethylammonium tetrafluoroborate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/jlac.198219820608