Technology Process of C18H17NO7
There total 11 articles about C18H17NO7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C21H23NO8;
With
toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol;
at 0 - 20 ℃;
With
sulfuric acid;
In
tetrahydrofuran; water;
at 0 - 20 ℃;
for 10h;
DOI:10.1002/anie.201006528
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydroxylamine hydrochloride; potassium carbonate / methanol; water / 1 h / 0 °C
2.1: N-chloro-succinimide; triethylamine / chloroform / 0 °C
3.1: toluene / 11 h / 20 °C
4.1: manganese(IV) oxide / toluene / 0.17 h / 80 °C
5.1: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 0 - 20 °C
5.2: 10 h / 0 - 20 °C
With
manganese(IV) oxide; N-chloro-succinimide; hydroxylamine hydrochloride; potassium carbonate; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; methanol; chloroform; water; toluene;
DOI:10.1002/anie.201006528
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-chloro-succinimide; triethylamine / chloroform / 0 °C
2.1: toluene / 11 h / 20 °C
3.1: manganese(IV) oxide / toluene / 0.17 h / 80 °C
4.1: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 0 - 20 °C
4.2: 10 h / 0 - 20 °C
With
manganese(IV) oxide; N-chloro-succinimide; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; methanol; chloroform; toluene;
DOI:10.1002/anie.201006528
