P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide

Base Information

Chemical Name:P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide
CAS No.:1613582-32-3
Molecular Formula:C₂₃H₂₄NOP
Molecular Weight:361.423
Hs Code.:

Synonyms:P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide

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Chemical Property of P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide

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Technology Process of P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide

There total 3 articles about P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 122333-71-5
trans-5-phenyl-4-penten-1-amine

: 1499-21-4
Diphenylphosphinic chloride

: 1613582-32-3
P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide

Guidance literature:: trans-5-phenyl-4-penten-1-amine; With 4-methyl-morpholine; In dichloromethane; at 0 ℃; Inert atmosphere; Schlenk technique;

Diphenylphosphinic chloride; In dichloromethane; at 0 - 20 ℃; for 5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ja5046296

Reference yield:

: 30154-22-4
trans-5-phenyl-4-pentenamide

: 1613582-32-3
P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

2.1: 4-methyl-morpholine / dichloromethane / 0 °C / Inert atmosphere; Schlenk technique

2.2: 5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With 4-methyl-morpholine; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja5046296

Reference yield:

: 22768-07-6,121746-04-1,93845-04-6
(E)-ethyl 5-phenylpent-4-enoate

: 1613582-32-3
P,P-diphenyl-N-((E)-5-phenylpent-4-enyl)phosphinicamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylaluminum; ammonium chloride / toluene / 55 °C / Schlenk technique; Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

3.1: 4-methyl-morpholine / dichloromethane / 0 °C / Inert atmosphere; Schlenk technique

3.2: 5 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With 4-methyl-morpholine; lithium aluminium tetrahydride; trimethylaluminum; ammonium chloride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja5046296