Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate

Base Information

Chemical Name:Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate
CAS No.:1176256-23-7
Molecular Formula:C₂₇H₃₂O₅
Molecular Weight:436.548
Hs Code.:

Synonyms:Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate

Suppliers and Price of Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate

There total 4 articles about Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.7%

: 25542-62-5
6-bromo-hexanoic acid ethyl ester

: 1176256-73-7
[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methanol

: 1176256-23-7
Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate

Guidance literature:: 6-bromo-hexanoic acid ethyl ester; [4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methanol; With phosphazene base-P₄-tert-butyl; In hexane; N,N-dimethyl-formamide; at 0 ℃; for 1h;

pH=7;

Reference yield:

: 321309-42-6
2-methyl-5-phenylfuran-3-carbaldehyde

: 1176256-23-7
Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / acetonitrile / -20 - 20 °C / Inert atmosphere

2.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / water; dimethyl sulfoxide / 4 h / 80 °C / Inert atmosphere

3.1: ethanol; sodium tetrahydroborate

4.1: phosphazene base-P₄-tert-butyl / N,N-dimethyl-formamide; hexane / 1 h / 0 °C

4.2: pH 7

With sodium tetrahydroborate; N-Bromosuccinimide; ethanol; sodium carbonate; phosphazene base-P₄-tert-butyl; bis-triphenylphosphine-palladium(II) chloride; In hexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1176256-71-5
4-bromo-2-methyl-5-phenylfuran-3-carbaldehyde

: 1176256-23-7
Ethyl 6-{[4-(4-methoxyphenyl)-2-methyl-5-phenylfuran-3-yl]methoxy}hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / water; dimethyl sulfoxide / 4 h / 80 °C / Inert atmosphere

2.1: ethanol; sodium tetrahydroborate

3.1: phosphazene base-P₄-tert-butyl / N,N-dimethyl-formamide; hexane / 1 h / 0 °C

3.2: pH 7

With sodium tetrahydroborate; ethanol; sodium carbonate; phosphazene base-P₄-tert-butyl; bis-triphenylphosphine-palladium(II) chloride; In hexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;