3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline

Base Information

Chemical Name:3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline
CAS No.:1014430-33-1
Molecular Formula:C₂₄H₂₄ClN₃O₄S
Molecular Weight:485.991
Hs Code.:

Synonyms:3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline

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Chemical Property of 3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline

Chemical Property:

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Technology Process of 3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline

There total 4 articles about 3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 554404-31-8
5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazole-2-thiol

: 35740-82-0
2-chloro-3-(bromomethyl)quinoline

: 1014430-33-1
3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.5012/jkcs.2011.55.4.656

Reference yield:

: 73568-25-9
2-chloro-3-quinoline carboxaldehyde

: 1014430-33-1
3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 20 °C

2: phosphorus tribromide / dichloromethane / 5 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.5012/jkcs.2011.55.4.656

Reference yield:

: 379254-36-1
3,4,5-triethoxybenzoic acid hydrazide

: 1014430-33-1
3-((5-(3,4,5-triethoxyphenyl)-1,3,4-oxadiazol-2-ylthio)methyl)-2-chloroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 8 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With potassium carbonate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.5012/jkcs.2011.55.4.656