3,4,5-Triethoxybenzohydrazide

Base Information

• Chemical Name: 3,4,5-Triethoxybenzohydrazide
• CAS No.: 379254-36-1
• Molecular Formula: C13H20 N2 O4
• Molecular Weight: 268.31
• Hs Code.: 2928000090
• DSSTox Substance ID: DTXSID70365835
• Wikidata: Q82150819
• Mol file: 379254-36-1.mol

Synonyms:3,4,5-triethoxybenzohydrazide;379254-36-1;Oprea1_227916;DTXSID70365835;BBL017855;MFCD03147243;STK487795;3,4,5-triethoxybenzoic acid hydrazide;AKOS000116234;SB86005;VS-06549;CS-0307620;EN300-03666;Z56922107

Chemical Property of 3,4,5-Triethoxybenzohydrazide

Chemical Property:

• Refractive Index: 1.521
• PSA: 82.81000
• Density: 1.125g/cm³
• LogP: 2.57740
• XLogP3: 1.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 7
• Exact Mass: 268.14230712
• Heavy Atom Count: 19
• Complexity: 259

Purity/Quality:

98%min ^*data from raw suppliers

3,4,5-Triethoxybenzohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC1=CC(=CC(=C1OCC)OCC)C(=O)NN

Technology Process of 3,4,5-Triethoxybenzohydrazide

There total 3 articles about 3,4,5-Triethoxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3,4,5-triethoxybenzoate (39666-77-8) → 3,4,5-triethoxybenzoic acid hydrazide (379254-36-1)

Guidance literature:

With hydrazine hydrate;

DOI:10.1002/ardp.19342721009

Reference yield:

3,4,5-trihydroxybenzoic acid (149-91-7) → 3,4,5-triethoxybenzoic acid hydrazide (379254-36-1)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH solution / anschliessendes Erwaermen mit wss. Natronlauge

2: sulfuric acid

3: hydrazine hydrate

With sodium hydroxide; sulfuric acid; hydrazine hydrate;

DOI:10.1002/ardp.19342721009

Reference yield:

3,4,5-triethoxybenzoic acid (6970-19-0) → 3,4,5-triethoxybenzoic acid hydrazide (379254-36-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid

2: hydrazine hydrate

With sulfuric acid; hydrazine hydrate;

DOI:10.1002/ardp.19342721009

upstream raw materials:

methyl 3,4,5-triethoxybenzoate

3,4,5-trihydroxybenzoic acid

3,4,5-triethoxybenzoic acid

Downstream raw materials:

N,N'-bis-(3,4,5-triethoxy-benzoyl)-hydrazine

3,4,5-triethoxy-benzoyl azide