2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid

Base Information

• Chemical Name: 2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid
• CAS No.: 748162-99-4
• Molecular Formula: C₁₇H₁₆Cl₂N₂O₆S
• Molecular Weight: 447.296

Synonyms:2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid

Chemical Property of 2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid

Chemical Property:

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Technology Process of 2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid

There total 1 articles about 2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(S)-benzyloxycarbonylamino-3-aminopropionic acid (18635-43-3) + 2,4-Dichlorobenzenesulfonyl chloride (16271-33-3) → 2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid (748162-99-4)

Guidance literature:

With citric acid; In 1,4-dioxane; sodium hydroxide;

Reference yield:

2-amino-3-(4-chlorophenyl)-N-(2.2-diethoxyethyl)-N-isopropyl-propionamide (746655-78-7) + 2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid (748162-99-4) → N-{2-(4-Chlorophenyl)-1-[(2,2-diethoxyethyl)isopropylcarbamoyl]ethyl}-3-(2,4-dichlorobenzenesulfonylamino)-2-methanesulfonylaminopropionamide

Guidance literature:

With N-ethylmorpholine;; benzotriazol-1-ol; 1,2-dichloro-ethane; In water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

2-amino-3-(4-chlorophenyl)-N-(2.2-diethoxyethyl)-N-(2,2-difluoroethyl)-propionamide (748164-43-4) + 2-benzyloxycarbonylamino-3-(2,4-dichlorobenzenesulfonylamino)-propanoic acid (748162-99-4) → benzyl [1-[2-(4-chlorophenyl)-1-[(2.2-diethoxyethyl)-(2,2-difluoroethyl)-carbamoyl]-ethylcarbamoyl]-2-(2,4-dichloro-benzenesulfonylamino)-ethyl]-carbamate (748164-44-5)

Guidance literature:

With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

upstream raw materials:

2-(S)-benzyloxycarbonylamino-3-aminopropionic acid

2,4-Dichlorobenzenesulfonyl chloride

Downstream raw materials:

benzyl [1-[2-(4-chlorophenyl)-1-[(2.2-diethoxyethyl)-(2,2-difluoroethyl)-carbamoyl]-ethylcarbamoyl]-2-(2,4-dichloro-benzenesulfonylamino)-ethyl]-carbamate

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