diisopropyl (E)-2-((((3aR,4R,6R₆aS)-6-(3-(4-methoxybenzyl)-2,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinylsulfonyl)methylsulfonyl)methylphosphonate

Base Information

• Chemical Name: diisopropyl (E)-2-((((3aR,4R,6R₆aS)-6-(3-(4-methoxybenzyl)-2,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinylsulfonyl)methylsulfonyl)methylphosphonate
• CAS No.: 1107654-51-2
• Molecular Formula: C₂₉H₄₁N₂O₁₃PS₂
• Molecular Weight: 720.756

Synonyms:diisopropyl (E)-2-((((3aR,4R,6R₆aS)-6-(3-(4-methoxybenzyl)-2,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinylsulfonyl)methylsulfonyl)methylphosphonate

Chemical Property of diisopropyl (E)-2-((((3aR,4R,6R₆aS)-6-(3-(4-methoxybenzyl)-2,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinylsulfonyl)methylsulfonyl)methylphosphonate

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Technology Process of diisopropyl (E)-2-((((3aR,4R,6R₆aS)-6-(3-(4-methoxybenzyl)-2,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinylsulfonyl)methylsulfonyl)methylphosphonate

There total 1 articles about diisopropyl (E)-2-((((3aR,4R,6R₆aS)-6-(3-(4-methoxybenzyl)-2,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinylsulfonyl)methylsulfonyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(3aR,4S,6R,6aS)-6-(3-(4-methoxybenzyl)-3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)-tetrahydro-2,2-dimethylfuro[3,4-d][1,3]dioxole-4-carbaldehyde (121845-98-5) + (diisopropoxyphosphorylmethanesulfonylmethanesulfonylmethyl)phosphonic acid diisopropyl ester (312512-49-5) → diisopropyl (E)-2-((((3aR,4R,6R6aS)-6-(3-(4-methoxybenzyl)-2,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)vinylsulfonyl)methylsulfonyl)methylphosphonate (1107654-51-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; lithium bromide; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/b819155g

upstream raw materials:

(3aR,4S,6R,6aS)-6-(3-(4-methoxybenzyl)-3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)-tetrahydro-2,2-dimethylfuro[3,4-d][1,3]dioxole-4-carbaldehyde

(diisopropoxyphosphorylmethanesulfonylmethanesulfonylmethyl)phosphonic acid diisopropyl ester

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