potassium (2R,3R)-1-(1-acetyl-2-methylprop-1-enyl)-4-oxo-3-phenoxyacetamidoazetidine-2-sulphinate

Base Information

Chemical Name:potassium (2R,3R)-1-(1-acetyl-2-methylprop-1-enyl)-4-oxo-3-phenoxyacetamidoazetidine-2-sulphinate
CAS No.:124597-97-3
Molecular Formula:C₁₇H₁₉N₂O₆S*K
Molecular Weight:418.512
Hs Code.:

Synonyms:potassium (2R,3R)-1-(1-acetyl-2-methylprop-1-enyl)-4-oxo-3-phenoxyacetamidoazetidine-2-sulphinate

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Chemical Property of potassium (2R,3R)-1-(1-acetyl-2-methylprop-1-enyl)-4-oxo-3-phenoxyacetamidoazetidine-2-sulphinate

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Technology Process of potassium (2R,3R)-1-(1-acetyl-2-methylprop-1-enyl)-4-oxo-3-phenoxyacetamidoazetidine-2-sulphinate

There total 2 articles about potassium (2R,3R)-1-(1-acetyl-2-methylprop-1-enyl)-4-oxo-3-phenoxyacetamidoazetidine-2-sulphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 124597-95-1
(3S,5R,6R)-3-acetyl-2,2-dimethyl-6-phenoxy-acetamidopenam 1,1-dioxide

: 124597-97-3
potassium (2R,3R)-1-(1-acetyl-2-methylprop-1-enyl)-4-oxo-3-phenoxyacetamidoazetidine-2-sulphinate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 1h;

Reference yield:

: 118693-29-1
(3S,5R,6R)-3-diazoacetyl-2,2-dimethyl-6-phenoxyacetamidopenam 1,1-dioxide

: 124597-97-3
potassium (2R,3R)-1-(1-acetyl-2-methylprop-1-enyl)-4-oxo-3-phenoxyacetamidoazetidine-2-sulphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 57percent hydroiodic acid / acetone / 0.25 h

2: 59 percent / potassium tert-butoxide / tetrahydrofuran / 1 h / -78 °C

With potassium tert-butylate; hydrogen iodide; In tetrahydrofuran; acetone;