C₃₈H₅₄N₂O₇SSi₂

Base Information

Chemical Name:C₃₈H₅₄N₂O₇SSi₂
CAS No.:1453217-97-4
Molecular Formula:C₃₈H₅₄N₂O₇SSi₂
Molecular Weight:739.093
Hs Code.:

C<sub>38</sub>H<sub>54</sub>N<sub>2</sub>O<sub>7</sub>SSi<sub>2</sub>

Synonyms:C₃₈H₅₄N₂O₇SSi₂

Suppliers and Price of C₃₈H₅₄N₂O₇SSi₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₈H₅₄N₂O₇SSi₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₈H₅₄N₂O₇SSi₂

There total 14 articles about C₃₈H₅₄N₂O₇SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1453217-96-3
C₃₄H₅₂O₇Si₂

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 1453217-97-4
C₃₈H₅₄N₂O₇SSi₂

Guidance literature:: With dmap; In dichloromethane; at 40 ℃; for 19h; Inert atmosphere;
DOI:10.1021/jo401170y

Reference yield:

: 1453217-91-8
1,2-O-isopropylidene-3-keto-4-C-(tert-butyldiphenylsilyl)oxymethyl-5-O-(tert-butyldimethylsilyl)-6-deoxy-6-C-vinyl-β-Lmannofuranose

: 1453217-97-4
C₃₈H₅₄N₂O₇SSi₂

Guidance literature:: Multi-step reaction with 4 steps

1: oxygen; copper diacetate; palladium dichloride / water; N,N-dimethyl acetamide / 24 h / 40 °C

2: L-proline / dimethyl sulfoxide / 54 h / 55 °C / Inert atmosphere

3: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 7 h / 0 - 23 °C / Inert atmosphere

4: dmap / dichloromethane / 19 h / 40 °C / Inert atmosphere

With dmap; oxygen; copper diacetate; acetic acid; L-proline; palladium dichloride; tetramethylammonium triacetoxyborohydride; In dichloromethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; acetonitrile; 2: |Aldol Condensation;
DOI:10.1021/jo401170y

Reference yield:

: 1453217-90-7
1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-4-C-(tert-butyldiphenylsilyl)oxymethyl-5-O-(tert-butyldimethylsilyl)-6-deoxy-6-C-vinyl-β-L-mannofuranose

: 1453217-97-4
C₃₈H₅₄N₂O₇SSi₂

Guidance literature:: Multi-step reaction with 6 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 6 h / 23 °C

2: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 18 h / 23 °C / Inert atmosphere

3: oxygen; copper diacetate; palladium dichloride / water; N,N-dimethyl acetamide / 24 h / 40 °C

4: L-proline / dimethyl sulfoxide / 54 h / 55 °C / Inert atmosphere

5: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 7 h / 0 - 23 °C / Inert atmosphere

6: dmap / dichloromethane / 19 h / 40 °C / Inert atmosphere

With dmap; oxygen; copper diacetate; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; L-proline; palladium dichloride; tetramethylammonium triacetoxyborohydride; In dichloromethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; acetonitrile; 2: |Wacker Oxidation / 4: |Aldol Condensation;
DOI:10.1021/jo401170y