C₃₄H₄₂N₂O₆Si

Base Information

Chemical Name:C₃₄H₄₂N₂O₆Si
CAS No.:1356491-84-3
Molecular Formula:C₃₄H₄₂N₂O₆Si
Molecular Weight:602.803
Hs Code.:

C<sub>34</sub>H<sub>42</sub>N<sub>2</sub>O<sub>6</sub>Si

Synonyms:C₃₄H₄₂N₂O₆Si

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Chemical Property of C₃₄H₄₂N₂O₆Si

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Technology Process of C₃₄H₄₂N₂O₆Si

There total 7 articles about C₃₄H₄₂N₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 98546-32-8
5-iodo-pyridine-2-carboxylic acid ethyl ester

: 1190391-64-0
4-methoxybenzyl {(1R)-1-[(R)-{[tert-butyl(dimethyl)silyl]oxy}(phenyl)methyl]pent-4-yn-1-yl}carbamate

: 1356491-84-3
C₃₄H₄₂N₂O₆Si

Guidance literature:: With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; at 55 ℃; for 5h; Inert atmosphere;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1356491-84-3
C₃₄H₄₂N₂O₆Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 4.17 h / 20 °C / Inert atmosphere

1.2: 1.5 h

1.3: pH 3

2.1: triethylamine; diphenyl phosphoryl azide / toluene / 5 h / 20 °C / Inert atmosphere

2.2: 16 h / 105 °C

3.1: triethylamine / copper(l) iodide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 5 h / 55 °C / Inert atmosphere

With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; In toluene; acetonitrile;

Reference yield:

: 53293-00-8
hex-5-ynoic acid

: 1356491-84-3
C₃₄H₄₂N₂O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine; pivaloyl chloride / tetrahydrofuran / 2.33 h / -25 °C / Inert atmosphere

1.2: 20 °C

2.1: chloro-trimethyl-silane; triethylamine; magnesium chloride / ethyl acetate / 72 h / 20 °C / Inert atmosphere

3.1: lithium hydroxide; dihydrogen peroxide / water; tetrahydrofuran / 0 - 5 °C

3.2: pH 3

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 4.17 h / 20 °C / Inert atmosphere

4.2: 1.5 h

4.3: pH 3

5.1: triethylamine; diphenyl phosphoryl azide / toluene / 5 h / 20 °C / Inert atmosphere

5.2: 16 h / 105 °C

6.1: triethylamine / copper(l) iodide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 5 h / 55 °C / Inert atmosphere

With chloro-trimethyl-silane; diphenyl phosphoryl azide; dihydrogen peroxide; pivaloyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; magnesium chloride; lithium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; In tetrahydrofuran; water; ethyl acetate; toluene; acetonitrile;