{5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid

Base Information

• Chemical Name: {5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid
• CAS No.: 850833-69-1
• Molecular Formula: C₄₇H₇₄N₄O₉
• Molecular Weight: 839.126

Synonyms:{5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid

Chemical Property of {5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid

Chemical Property:

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Technology Process of {5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid

There total 1 articles about {5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C85H126N8O19 → 8-hydroxy-oct-5-enoic acid + N-[(3-hexanoylamino-phenylcarbamoyl)-methyl]-5-(2-hydroxy-acetylamino)-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-benzamide (850833-76-0) + {5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid (850833-69-1)

Guidance literature:

With sodium hydroxide; In acetone; at 20 ℃; for 6h;

DOI:10.1002/anie.200461777

Reference yield: 90.0%

{5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid (850833-69-1) + allyl alcohol (107-18-6) → {5-[2-(5-butylcarbamoyl-2,4-bis-octyloxy-benzoylamino)-acetylamino]-2-octyloxy-benzoylamino}-acetic acid allyl ester (850833-73-7)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 24h;

DOI:10.1002/anie.200461777

Reference yield: 88.0%

{5-[2-(5-butylcarbamoyl-2,4-bis-ctyloxy-benzoylamino)-acetylamino]-2-octyloxybenzoylamino}-acetic acid (850833-69-1) + o-Allylphenol (1745-81-9) → {5-[2-(5-butylcarbamoyl-2,4-bis-octyloxy-benzoylamino)-acetylamino]-2-octyloxy-benzoylamino}-acetic acid 2-allyl-phenyl ester (850833-75-9)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 24h;

DOI:10.1002/anie.200461777

Downstream raw materials:

{5-[2-(5-butylcarbamoyl-2,4-bis-octyloxy-benzoylamino)-acetylamino]-2-octyloxy-benzoylamino}-acetic acid 1-methyl-allyl ester

{5-[2-(5-butylcarbamoyl-2,4-bis-octyloxy-benzoylamino)-acetylamino]-2-octyloxy-benzoylamino}-acetic acid pent-4-enyl ester

{5-[2-(5-butylcarbamoyl-2,4-bis-octyloxy-benzoylamino)-acetylamino]-2-octyloxy-benzoylamino}-acetic acid but-3-enyl ester

{5-[2-(5-butylcarbamoyl-2,4-bis-octyloxy-benzoylamino)-acetylamino]-2-octyloxy-benzoylamino}-acetic acid allyl ester

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