1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Base Information

Chemical Name:1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene
CAS No.:137022-85-6
Molecular Formula:C₂₁H₃₀N₂O₄Si
Molecular Weight:402.566
Hs Code.:

Synonyms:1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

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Chemical Property of 1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Chemical Property:

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Technology Process of 1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

There total 11 articles about 1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (3,4-Dimethoxy-5-{[1-phenyl-meth-(E)-ylidene]-amino}-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

: 137022-85-6
1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Guidance literature:: With sodium cyanoborohydride; In acetonitrile; at 50 - 60 ℃; Yield given;
DOI:10.1016/S0040-4039(00)79889-3

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 137022-85-6
1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 2 h / 60 °C

2: 100 percent / hydrogen / 10percent Pd-C / ethanol / 2 h

3: acetonitrile / 1 h

4: NaBH₃CN / acetonitrile / 12 h / 50 °C

With hydrogen; sodium cyanoborohydride; palladium on activated charcoal; In ethanol; toluene; acetonitrile;
DOI:10.1016/S0040-4020(01)85065-1

Reference yield:

: 22027-96-9
5-nitroveratral

: 137022-85-6
1-benzylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Guidance literature:: Multi-step reaction with 10 steps

1: iron dust, 12 M HCl / methanol / 10 h / Heating

2: Na₂CO₃ / diethyl ether; H₂O / 1.) 0 deg C, 30 min; 2.) room temp., 2 h

3: 93 percent / Jones reagent / acetone / 1.) 0 deg C, 30 min; 2.) room temp., 1 h

4: tetrahydrofuran / 2 h / Ambient temperature

5: 2 M aq. NaN₃ / tetrahydrofuran; H₂O / 2 h / Ambient temperature

6: toluene / 0.5 h / Heating

7: toluene / 2 h / 60 °C

8: 100 percent / hydrogen / 10percent Pd-C / ethanol / 2 h

9: acetonitrile / 1 h

10: NaBH₃CN / acetonitrile / 12 h / 50 °C

With hydrogenchloride; sodium azide; jones reagent; hydrogen; iron; sodium cyanoborohydride; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; acetone; toluene; acetonitrile;
DOI:10.1016/S0040-4020(01)85065-1