(2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran

Base Information

• Chemical Name: (2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran
• CAS No.: 285994-43-6
• Molecular Formula: C₃₆H₄₀N₁₂O₇
• Molecular Weight: 752.79

Synonyms:(2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran

Chemical Property of (2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran

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Technology Process of (2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran

There total 1 articles about (2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-glycidyl tosylate (113826-06-5,6746-81-2) + 1,3,2',6'-tetraazido-6,3',4'-tri-O-benzyl neamine (236115-80-3) → (2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran (285994-43-6)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2005.02.029

Reference yield: 90.0%

(2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran (285994-43-6) + N,N`-dimethylethylenediamine (110-70-3) → C76H92N26O14

Guidance literature:

In ethanol; at 95 ℃; for 16h;

DOI:10.1021/ja000575w

Reference yield: 77.9%

1,3-bis(methylamino)propane (111-33-1) + (2R,3R,4R,5R,6R)-3-Azido-6-azidomethyl-4,5-bis-benzyloxy-2-[(1R,2R,3S,4R,6S)-4,6-diazido-3-benzyloxy-2-((R)-1-oxiranylmethoxy)-cyclohexyloxy]-tetrahydro-pyran (285994-43-6) → C77H94N26O14

Guidance literature:

In ethanol; at 95 ℃; for 16h;

DOI:10.1021/ja000575w

upstream raw materials:

(R)-glycidyl tosylate

1,3,2',6'-tetraazido-6,3',4'-tri-O-benzyl neamine

Downstream raw materials:

C₇₈H₉₆N₂₆O₁₄

(R)-1-[(1R,2R,3S,5R,6S)-3,5-Diazido-2-((2R,3R,4R,5R,6R)-3-azido-6-azidomethyl-4,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-6-benzyloxy-cyclohexyloxy]-3-methylamino-propan-2-ol

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