C₅₅H₇₁IO₅

Base Information

Chemical Name:C₅₅H₇₁IO₅
CAS No.:1256563-92-4
Molecular Formula:C₅₅H₇₁IO₅
Molecular Weight:939.07
Hs Code.:

C<sub>55</sub>H<sub>71</sub>IO<sub>5</sub>

Synonyms:C₅₅H₇₁IO₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₅H₇₁IO₅

Chemical Property:

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Technology Process of C₅₅H₇₁IO₅

There total 11 articles about C₅₅H₇₁IO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1791-26-0
4-vinyl-benzaldehyde

: 1256563-91-3
C₄₈H₆₇IO₄

: 1256563-92-4
C₅₅H₇₁IO₅

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In chloroform; benzene; for 48h; stereospecific reaction; Inert atmosphere; Reflux;
DOI:10.1021/ol102398y

Reference yield:

: 111-25-1
1-bromo-hexane

: 1256563-92-4
C₅₅H₇₁IO₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydrosulfite pentahydrate; tetrabutylammomium bromide; potassium hydroxide / water; toluene / Cooling with ice; Reflux

2.1: Iodine monochloride / methanol / Cooling with ice; Reflux

3.1: n-butyllithium / diethyl ether; hexane / 0.75 h / 0 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / diethyl ether; hexane / 0 °C / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform / 40 h / Inert atmosphere; Reflux

7.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 0 - 20 °C / Inert atmosphere

8.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform; benzene / 48 h / Inert atmosphere; Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; n-butyllithium; sodium hydrosulfite pentahydrate; potassium tert-butylate; tetrabutylammomium bromide; Iodine monochloride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; water; toluene; benzene; 4.1: Wittig reaction / 7.1: Wittig reaction / 7.2: Wittig reaction;
DOI:10.1021/ol102398y

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 1256563-92-4
C₅₅H₇₁IO₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydrosulfite pentahydrate; tetrabutylammomium bromide; potassium hydroxide / water; toluene / Cooling with ice; Reflux

2.1: Iodine monochloride / methanol / Cooling with ice; Reflux

3.1: n-butyllithium / diethyl ether; hexane / 0.75 h / 0 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / diethyl ether; hexane / 0 °C / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform / 40 h / Inert atmosphere; Reflux

7.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 0 - 20 °C / Inert atmosphere

8.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform; benzene / 48 h / Inert atmosphere; Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; n-butyllithium; sodium hydrosulfite pentahydrate; potassium tert-butylate; tetrabutylammomium bromide; Iodine monochloride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; water; toluene; benzene; 4.1: Wittig reaction / 7.1: Wittig reaction / 7.2: Wittig reaction;
DOI:10.1021/ol102398y