C₃₁H₄₂O₆S₂

Base Information

Chemical Name:C₃₁H₄₂O₆S₂
CAS No.:537658-35-8
Molecular Formula:C₃₁H₄₂O₆S₂
Molecular Weight:574.803
Hs Code.:

C<sub>31</sub>H<sub>42</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₃₁H₄₂O₆S₂

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Chemical Property of C₃₁H₄₂O₆S₂

Chemical Property:

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Technology Process of C₃₁H₄₂O₆S₂

There total 14 articles about C₃₁H₄₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 537658-33-6
C₃₁H₄₀O₆S₂

: 537658-35-8
C₃₁H₄₂O₆S₂

Guidance literature:: With magnesium; In methanol; at 80 ℃; for 2h;
DOI:10.1021/ol034218c

Reference yield:

: 100-39-0
benzyl bromide

: 537658-35-8
C₃₁H₄₂O₆S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: 78 percent / NaH; Bu₄NI / dimethylformamide / 1 h / 0 - 20 °C

2.1: 75 percent / n-BuLi / tetrahydrofuran; hexane / 0 - 20 °C

3.1: O₃ / CH₂Cl₂; methanol / 0.08 h / -78 °C

3.2: 75 percent / Me₂S / CH₂Cl₂; methanol / 14 h / -78 - 20 °C

4.1: 75 percent / MgBr₂; Et₃N / tetrahydrofuran / 2.5 h

5.1: 100 percent / HF / acetonitrile / 24 h / 20 °C

6.1: 63 percent / DMAP; Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

7.1: toluene / 24 h / 200 °C

8.1: K₂CO₃ / CH₂Cl₂; methanol / 14 h / 20 °C

9.1: 80 percent / NaBH₄ / tetrahydrofuran; H₂O / 16 h / 70 °C

10.1: Mg / methanol / 2 h / 80 °C

With dmap; sodium tetrahydroborate; n-butyllithium; hydrogen fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; ozone; magnesium; triethylamine; magnesium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 4.1: modified Horner-Wadsworth-Emmons reaction / 7.1: intramolecular Diels-Alder reaction;
DOI:10.1021/ol034218c

Reference yield:

: 124957-46-6
(2E,4E)-methyl 2-acetoxymethyl-5-phenyl-penta-2,4-dienoate

: 537658-35-8
C₃₁H₄₂O₆S₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 100 percent / K₂CO₃ / methanol / 4 h / 20 °C

2.1: 78 percent / NaH; Bu₄NI / dimethylformamide / 1 h / 0 - 20 °C

3.1: 75 percent / n-BuLi / tetrahydrofuran; hexane / 0 - 20 °C

4.1: O₃ / CH₂Cl₂; methanol / 0.08 h / -78 °C

4.2: 75 percent / Me₂S / CH₂Cl₂; methanol / 14 h / -78 - 20 °C

5.1: 75 percent / MgBr₂; Et₃N / tetrahydrofuran / 2.5 h

6.1: 100 percent / HF / acetonitrile / 24 h / 20 °C

7.1: 63 percent / DMAP; Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

8.1: toluene / 24 h / 200 °C

9.1: K₂CO₃ / CH₂Cl₂; methanol / 14 h / 20 °C

10.1: 80 percent / NaBH₄ / tetrahydrofuran; H₂O / 16 h / 70 °C

11.1: Mg / methanol / 2 h / 80 °C

With dmap; sodium tetrahydroborate; n-butyllithium; hydrogen fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; ozone; magnesium; triethylamine; magnesium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 5.1: modified Horner-Wadsworth-Emmons reaction / 8.1: intramolecular Diels-Alder reaction;
DOI:10.1021/ol034218c