benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate

Base Information

Chemical Name:benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate
CAS No.:149401-94-5
Molecular Formula:C₆₀H₅₇N₃O₁₈S₃
Molecular Weight:1204.32
Hs Code.:

Synonyms:benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate

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Chemical Property of benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate

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Technology Process of benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate

There total 1 articles about benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 18226-42-1
1,3,5-Tris(bromomethyl)benzene

: 149401-93-4
5-(Tosylamino)isophthalsaeure-dimethylester

: 149401-94-5
benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 4h;

Reference yield: 49.0%

: 149401-94-5
benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate

: 149401-96-7
benzene<3-1,3,5>:<5--1,3-phenylene>:methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;

Reference yield:

: 149401-94-5
benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:methyl carboxylate

: 149401-98-9
benzene<3-1,3,5>:<5-(N-tosyl-1-azaethyl)-1,3-phenylene>:bromomethane

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

2: 55 percent / PBr₃ / CHCl₃ / 1) reflux, 2 h, 2) r.t., 12 h

With lithium aluminium tetrahydride; phosphorus tribromide; In tetrahydrofuran; chloroform;