(η-cyclopentadienyl)((2,3-diphenyl-2-cyclopropen-1-yl)carbonyl)dicarbonyliron

Base Information

Chemical Name:(η-cyclopentadienyl)((2,3-diphenyl-2-cyclopropen-1-yl)carbonyl)dicarbonyliron
CAS No.:69302-82-5
Molecular Formula:C₂₃H₁₆FeO₃
Molecular Weight:396.225
Hs Code.:

Synonyms:(η-cyclopentadienyl)((2,3-diphenyl-2-cyclopropen-1-yl)carbonyl)dicarbonyliron

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Chemical Property of (η-cyclopentadienyl)((2,3-diphenyl-2-cyclopropen-1-yl)carbonyl)dicarbonyliron

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Technology Process of (η-cyclopentadienyl)((2,3-diphenyl-2-cyclopropen-1-yl)carbonyl)dicarbonyliron

There total 1 articles about (η-cyclopentadienyl)((2,3-diphenyl-2-cyclopropen-1-yl)carbonyl)dicarbonyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: sodium dicarbonyl(cyclopentadienyl)ferrate

: 6415-58-3
2,3-diphenyl-2-cyclopropene-1-carbonyl chloride

: 69302-82-5
(η-cyclopentadienyl)((2,3-diphenyl-2-cyclopropen-1-yl)carbonyl)dicarbonyliron

Guidance literature:: In tetrahydrofuran; soln. of Fe-complex in THF was filtered, cooled to -78°C, soln. of ligand in THF was added dropwise under N2, mixt. was stirred for 1 h at -78°C, warmed to ambient temp.; THF was removed under vac., residue extd. with CH2Cl2, filtered, evapd.to dryness, chromd. on florisil/hexane column, evapd. to dryness, recrystd. from CH2Cl2/hexane (-30°);
DOI:10.1021/ja00382a018