8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester

Base Information

• Chemical Name: 8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester
• CAS No.: 104576-52-5
• Molecular Formula: C₂₆H₂₇N₅O₆
• Molecular Weight: 505.53

Synonyms:8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester

Chemical Property of 8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester

Chemical Property:

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Technology Process of 8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester

There total 2 articles about 8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyl 2-(4-aminophenyl)acetate hydrochloride (83528-16-9) + [4-(1,3-Diethyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid (104576-44-5) → 8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester (104576-52-5)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;

DOI:10.1021/jm00384a037

Reference yield:

→ 8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester (104576-52-5)

Guidance literature:

Reference yield: 77.0%

8-<4-<<<<4-(carboxymethyl)anilino>carbonyl>methyl>oxy>phenyl>-1,3-diethylxanthine methyl ester (104576-52-5) + ethylenediamine (107-15-3,85404-18-8) → N-{4-[(2-Amino-ethylcarbamoyl)-methyl]-phenyl}-2-[4-(1,3-diethyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetamide (104576-54-7)

Guidance literature:

at 50 ℃;

DOI:10.1021/jm00384a037

upstream raw materials:

methyl 2-(4-aminophenyl)acetate hydrochloride

[4-(1,3-Diethyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetic acid

Downstream raw materials:

N-{4-[(2-Amino-ethylcarbamoyl)-methyl]-phenyl}-2-[4-(1,3-diethyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetamide

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