tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾

Base Information

Chemical Name:tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾
CAS No.:121191-92-2
Molecular Formula:C₂₂H₃₉NiP
Molecular Weight:393.215
Hs Code.:

tricyclohexylphosphane(ethene)(ethyne)nickel<sup>(0)</sup>

Synonyms:tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾

Chemical Property:

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Technology Process of tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾

There total 2 articles about tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50696-82-7
tris(ethene)nickel⁽⁰⁾

: 74-86-2,25067-58-7
acetylene

: 2622-14-2
tricyclohexylphosphine

: 121191-92-2
tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾

Guidance literature:: In diethyl ether; yellow cryst. product of Ni-complex and ethyne in ether treated with the phosphane below -100°C under Ar (Schlenk-type glassware);
DOI:10.1021/ja00197a029

Reference yield:

: 33152-09-9
(CH₂CH₂)2NiP(C₆H₁₁-cyclo)3

: 74-86-2,25067-58-7
acetylene

: 2622-14-2
tricyclohexylphosphine

: 121191-92-2
tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾

Guidance literature:: In diethyl ether; solid Ni-complex suspended in ether, ethyne added at -78°C under Ar (Schlenk-type glassware);
DOI:10.1021/ja00197a029

Reference yield: 83.0%

: 121191-92-2
tricyclohexylphosphane(ethene)(ethyne)nickel⁽⁰⁾

: 23936-60-9
1,2-bis(dimethylphosphanyl)ethane

: 121192-06-1
((CH₃)2PCH₂CH₂P(CH₃)2){((C₆H₁₁)3P)Ni(CHCH)}2

Guidance literature:: In diethyl ether; ethereal soln. of Ni-complex combined with dmpe in ether at -30°C under Ar; crystn. (kept at -78°C overnight), mother liquor drained off through a capillary, washed (cold pentane), dried (vac., -30°C), elem. anal.;
DOI:10.1021/ja00197a029