tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane

Base Information

Chemical Name:tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane
CAS No.:1374036-51-7
Molecular Formula:C₃₀H₃₈O₄Si
Molecular Weight:490.715
Hs Code.:

Synonyms:tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane

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Chemical Property of tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane

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Technology Process of tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane

There total 9 articles about tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1374036-50-6
C₃₇H₄₆O₇SSi

: 1374036-51-7
tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane

Guidance literature:: With potassium carbonate; In methanol; at 0 - 20 ℃; for 0.5h;
DOI:10.1039/c2ob25151e

Reference yield:

: 1374036-46-0
(4S)-4-(((S)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl)-2-(4-methoxyphenyl)-1,3-dioxane

: 1374036-51-7
tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / 0 - 20 °C

2: 1H-imidazole / dichloromethane / 5 h / 0 - 20 °C

3: copper(II) choride dihydrate / acetonitrile / 0.5 h / 0 - 20 °C

4: di(n-butyl)tin oxide; triethylamine / dichloromethane / 1 h / 0 - 20 °C

5: potassium carbonate / methanol / 0.5 h / 0 - 20 °C

With 1H-imidazole; copper(II) choride dihydrate; diisobutylaluminium hydride; di(n-butyl)tin oxide; potassium carbonate; triethylamine; In methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1039/c2ob25151e

Reference yield:

: 1374036-48-2
tert-butyl((S)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-3-(4-methoxybenzyloxy)butoxy)diphenylsilane

: 1374036-51-7
tert.-butyl((S)-3-(4-methoxybenzyloxy)-4-((S)-oxiran-2-yl)butoxy)diphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: copper(II) choride dihydrate / acetonitrile / 0.5 h / 0 - 20 °C

2: di(n-butyl)tin oxide; triethylamine / dichloromethane / 1 h / 0 - 20 °C

3: potassium carbonate / methanol / 0.5 h / 0 - 20 °C

With copper(II) choride dihydrate; di(n-butyl)tin oxide; potassium carbonate; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1039/c2ob25151e