(3R,4S,14R,15R,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine

Base Information

Chemical Name:(3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine
CAS No.:95464-02-1
Molecular Formula:C₂₁H₂₆N₂O₃
Molecular Weight:354.449
Hs Code.:

Synonyms:(3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine

Suppliers and Price of (3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine

Chemical Property:

Purity/Quality:

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Technology Process of (3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine

There total 1 articles about (3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96-34-4
methyl chloroacetate

: 51152-47-7
(1R*,5S*,12bS*)-1-ethyl-1,2,3,4,6,7,12,12b-octahydroindolo<2,3-a>quinolizine-1-carbaldehyde

: 4880-92-6,38990-18-0,51773-19-4,56942-60-0,78341-04-5,89825-94-5
(+/-)-apovincamine

: 95464-02-1
(3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine

Guidance literature:: With potassium tert-butylate; In benzene; for 0.333333h; Ambient temperature;

Reference yield:

: 95464-02-1
(3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine

: 27773-65-5
Apovincaminic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

2: 55 percent / DBU / 1 h / 100 °C

3: aq. NaOH / methanol; tetrahydrofuran / 12 h

With sodium hydroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo00208a017

Reference yield:

: 95464-02-1
(3R*,4S*,14R*,15R*,16S*)-14,15-dihydro-15-hydroxy-14-methoxycarbonyleburnamenine

: 4880-92-6
apovincamine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

2: 55 percent / DBU / 1 h / 100 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In dichloromethane;
DOI:10.1021/jo00208a017