5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester

Base Information

Chemical Name:5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester
CAS No.:477587-07-8
Molecular Formula:C₃₀H₅₅NO₅SSi
Molecular Weight:569.922
Hs Code.:

Synonyms:5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester

Suppliers and Price of 5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester

There total 4 articles about 5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 220315-20-8
(R,E)-2-methyl-N-(3-methylbutylidene)-2-propanesulfinamide

: 477587-06-7
4-(triisopropylsilanyloxy)butyric acid 4-methoxybenzyl ester

: 477587-07-8
5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester

Guidance literature:: 4-(triisopropylsilanyloxy)butyric acid 4-methoxybenzyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h;

With triisopropoxytitanium(IV) chloride; In tetrahydrofuran; at -78 ℃; for 0.5h;

(R,E)-2-methyl-N-(3-methylbutylidene)-2-propanesulfinamide; In tetrahydrofuran; at -78 ℃; for 3h; Further stages.;
DOI:10.1021/jo025957u

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 477587-07-8
5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 71 percent / imidazole / tetrahydrofuran / 24 h / 20 °C

2.1: lithium diisopropylamide / tetrahydrofuran / 0.5 h / -78 °C

2.2: titanium triisopropoxide chloride / tetrahydrofuran / 0.5 h / -78 °C

2.3: tetrahydrofuran / 3 h / -78 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jo025957u

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 477587-07-8
5-methyl-3-(2-methylpropane-2-sulfinylamino)-2-(2-(triisopropylsilanyloxy)ethyl)hexanoic acid 4-methoxybenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutylammonium iodide / acetone / 24 h / Heating

2.1: 71 percent / imidazole / tetrahydrofuran / 24 h / 20 °C

3.1: lithium diisopropylamide / tetrahydrofuran / 0.5 h / -78 °C

3.2: titanium triisopropoxide chloride / tetrahydrofuran / 0.5 h / -78 °C

3.3: tetrahydrofuran / 3 h / -78 °C

With 1H-imidazole; tetra-(n-butyl)ammonium iodide; lithium diisopropyl amide; In tetrahydrofuran; acetone;
DOI:10.1021/jo025957u