Technology Process of C39H30N2S
There total 6 articles about C39H30N2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; water;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 20 h / 85 °C / Inert atmosphere
2: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / Inert atmosphere; Reflux
With
potassium acetate; sodium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,4-dioxane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxygen / palladium 10% on activated carbon / ethanol / 144 h / Reflux
2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 20 h / 85 °C / Inert atmosphere
3: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; tetrahydrofuran / Inert atmosphere; Reflux
With
oxygen; potassium acetate; sodium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water;