5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole

Base Information

• Chemical Name: 5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole
• CAS No.: 1045600-98-3
• Molecular Formula: C₂₅H₂₃N₃O₂
• Molecular Weight: 397.477

Synonyms:5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole

Chemical Property of 5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole

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Technology Process of 5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole

There total 1 articles about 5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5,6-dimethyl-9-methoxy-1-(2'-methoxy-4'-nitro)phenyl-6H-pyrido[4,3-b]carbazole (1045600-96-1) → 5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole (1045600-98-3)

Guidance literature:

With palladium 10% on activated carbon; In acetic acid; at 50 ℃; for 1h;

DOI:10.1002/ardp.200700203

Reference yield: 84.0%

5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole (1045600-98-3) + methanesulfonyl chloride (124-63-0) → 5,6-dimethyl-9-methoxy-1-(4'-mathanesulfamoyl-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole (1045601-03-3)

Guidance literature:

5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole; With dmap; In chloroform; for 0.5h;

methanesulfonyl chloride; In chloroform; at 20 ℃; for 24h;

DOI:10.1002/ardp.200700203

Reference yield: 82.0%

5,6-dimethyl-9-methoxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole (1045600-98-3) + acetic anhydride (108-24-7) → 5,6-dimethyl-9-methoxy-1-(4'-acetamido-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole (1045601-02-2)

Guidance literature:

With pyridine; at 20 ℃; for 2h;

DOI:10.1002/ardp.200700203

upstream raw materials:

5,6-dimethyl-9-methoxy-1-(2'-methoxy-4'-nitro)phenyl-6H-pyrido[4,3-b]carbazole

Downstream raw materials:

5,6-dimethyl-9-hydroxy-1-(4'-amino-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole

5,6-dimethyl-9-methoxy-1-(4'-acetamido-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole

5,6-dimethyl-9-methoxy-1-(4'-mathanesulfamoyl-2'-methoxy)phenyl-6H-pyrido[4,3-b]carbazole

5,6-dimethyl-9-methoxy-1-[2'-methoxy-4'-(3-methylureilene)]phenyl-6H-pyrido[4,3-b]carbazole

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