[(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid

Base Information

• Chemical Name: [(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid
• CAS No.: 1072833-70-5
• Molecular Formula: C₁₄H₂₀BBrN₂O₄
• Molecular Weight: 371.039

Synonyms:[(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid

Chemical Property of [(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid

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Technology Process of [(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid

There total 7 articles about [(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide (1072833-91-0) → [(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid (1072833-70-5)

Guidance literature:

With hydrogenchloride; Dihydroxy-isobutyl-boran; water; In methanol; hexane;

Reference yield: 73.0%

Dihydroxy-isobutyl-boran (84110-40-7) + 2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethylhexahydro-4,6-methano-1,3,2-benzodioxaborol-2-yl]butyl}amino)-2-oxoethyl]benzamide → [(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid (1072833-70-5)

Guidance literature:

With hydrogenchloride; water; In methanol; hexane;

Reference yield:

2-bromo-N-[2-({(1R)-3-methyl-1-[(3aR,4R,6R,7aS)-3a,5,5-trimethylhexahydro-4,6-methano-1,3,2-benzodioxaborol-2-yl]butyl}amino)-2-oxoethyl]benzamide → [(1R)-1-({[(2-bromobenzoyl)amino]acetyl}amino)-3-methylbutyl]boronic acid (1072833-70-5)

Guidance literature:

With methanol; Dihydroxy-isobutyl-boran; In methanol; hexane;

upstream raw materials:

Dihydroxy-isobutyl-boran

2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide

(aR,3aS,4S,6S,7aR)-hexahydro-3a,8,8-trimethyl-α-(2-methylpropyl)-4,6-methano-1,3,2-benzodioxaborole-2-methanamine 2,2,2-trifluoroacetate

tert-butyl [2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)-2-oxoethyl]carbamate

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