2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide

Base Information

Chemical Name:2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide
CAS No.:1072833-91-0
Molecular Formula:C₂₄H₃₄BBrN₂O₄
Molecular Weight:505.26
Hs Code.:

Synonyms:2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide

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Chemical Property of 2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide

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Technology Process of 2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide

There total 4 articles about 2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 847494-22-8
2-amino-N-{(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethylhexahydro-4,6-methano-1,3,2-benzodioxaborol-2-yl]butyl}acetamide monohydrochloride

: 88-65-3
2-bromobenzoic-acid

: 1072833-91-0
2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 2h;

Reference yield: 78.0%

: 2-amino-N-{(1R)-3-methyl-1-[(3aS,4S,6S,7AR)-3a,5,5-trimethylhexahydro-4,6-methano-1,3,2-benzodioxaborol-2-yl]butyl}acetamide hydrochloride

: 88-65-3
2-bromobenzoic-acid

: 1072833-91-0
2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 2h;

Reference yield:

: 1310383-72-2,179324-87-9
(aR,3aS,4S,6S,7aR)-hexahydro-3a,8,8-trimethyl-α-(2-methylpropyl)-4,6-methano-1,3,2-benzodioxaborole-2-methanamine 2,2,2-trifluoroacetate

: 1072833-91-0
2-bromo-N-[2-({(1R)-3-methyl-1-[(3aS,4S,6S,7aR)-3a,5,5-trimethyl hexahydro-4,6-methano-1,3,2-benzodioxaborole-2-yl]butyl}amino)2-oxoethyl]benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane

2: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / 2 h

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane;