5-phenyltropolone

Base Information

Chemical Name:5-phenyltropolone
CAS No.:15796-71-1
Molecular Formula:C₁₃H₁₀O₂
Molecular Weight:198.221
Hs Code.:

Synonyms:5-phenyltropolone

Suppliers and Price of 5-phenyltropolone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-phenyltropolone

Chemical Property:

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Technology Process of 5-phenyltropolone

There total 15 articles about 5-phenyltropolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 3172-00-7
5-bromotropolone

: 98-80-6
phenylboronic acid

: 15796-71-1
5-phenyltropolone

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 48h; Inert atmosphere; Reflux;
DOI:10.1246/bcsj.82.236

Reference yield: 61.0%

: (1S,2R,5S)-2-Hydroxy-6-phenyl-8-oxa-bicyclo[3.2.1]oct-6-en-3-one

: 15796-71-1
5-phenyltropolone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; triethylamine;
DOI:10.1016/S0040-4039(99)01589-0

Reference yield:

: 107752-52-3
2-amino-5-(4-aminophenyl)tropone

: 15796-71-1
5-phenyltropolone

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 6M KOH / ethanol / Heating

2: 1.) nitrous acid; 2.) phosphinic acid

With potassium hydroxide; hypophosphorous acid; cis-nitrous acid; In ethanol;
DOI:10.1246/bcsj.62.128