2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol

Base Information

Chemical Name:2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol
CAS No.:692205-65-5
Molecular Formula:C₃₀H₃₉BrO₄
Molecular Weight:543.541
Hs Code.:

Synonyms:2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol

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Chemical Property of 2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol

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Technology Process of 2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol

There total 6 articles about 2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 692205-60-0
[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-acetic acid ethyl ester

: 692205-65-5
2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; for 8h; Heating;
DOI:10.1021/jo049878p

Reference yield:

: 2050-77-3
Iododecane

: 692205-65-5
2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

2: 63 percent / sodium hydride; 18-crown-6 / tetrahydrofuran / 20 °C

3: 81 percent / borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

With 18-crown-6 ether; dimethylsulfide borane complex; sodium hydride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1021/jo049878p

Reference yield:

: 350035-53-9
3,5-dihydroxy-4-bromobenzoic acid ethyl ester

: 692205-65-5
2-[2-bromo-3-decyloxy-5-(naphthalen-2-ylmethoxymethyl)-phenoxy]-ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: 27 percent / LiAlH₄ / tetrahydrofuran / 2 h

2: 84 percent / potassium carbonate; potassium iodide; 18-crown-6 / acetone / 6 h / Heating

3: potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

4: 63 percent / sodium hydride; 18-crown-6 / tetrahydrofuran / 20 °C

5: 81 percent / borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

With lithium aluminium tetrahydride; 18-crown-6 ether; dimethylsulfide borane complex; sodium hydride; potassium carbonate; potassium iodide; In tetrahydrofuran; acetone;
DOI:10.1021/jo049878p