N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide

Base Information

Chemical Name:N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide
CAS No.:191864-44-5
Molecular Formula:C₁₂H₁₅ClN₂O₃
Molecular Weight:270.716
Hs Code.:

Synonyms:N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide

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Technology Process of N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide

There total 1 articles about N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 29968-78-3
2-(4-nitrophenyl)ethylamine monohydrochloride

: 4635-59-0
4-Chlorobutanoyl chloride

: 191864-44-5
N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide

Guidance literature:: With triethylamine; In tetrahydrofuran; for 48h; Ambient temperature;
DOI:10.1021/jm9605849

Reference yield: 22.0%

: 191864-44-5
N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide

: 26340-10-3
N-[2-(4-nitrophenyl)ethyl]-2-pyrrolidinone

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; for 24h; Heating;
DOI:10.1021/jm9605849

Reference yield:

: 191864-44-5
N-[2-(4-nitrophenyl)ethyl]-4-chlorobutylamide

: N-[2-(4-nitrophenyl)ethyl]-2-pyrrolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 22 percent / 5 N aq. NaOH / tetrahydrofuran / 24 h / Heating

2: 90 percent / H₂, aq. HCl / 10percent Pd/C / ethanol / 760 Torr / Ambient temperature

With hydrogenchloride; sodium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm9605849