2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside
CAS No.:1595122-13-6
Molecular Formula:C₅₀H₅₆O₁₆SeSi
Molecular Weight:1020.03
Hs Code.:

2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside

Synonyms:2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside

There total 11 articles about 2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1595121-91-7
2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-β-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 1595122-13-6
2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 24h; Cooling with ice; Inert atmosphere;
DOI:10.1016/j.bmc.2014.02.023

Reference yield:

: 1595121-53-1
2-(trimethylsilyl)ethyl 2,3-di-O-(p-methoxybenzyl)-β-D-glucopyranoside

: 1595122-13-6
2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 8 h / -40 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

2.2: 3 h / -40 °C / Inert atmosphere; Molecular sieve

3.1: trifluoroacetic acid / dichloromethane / 2.5 h / -20 °C / Inert atmosphere

4.1: pyridine / 24 h / 20 °C / Cooling with ice; Inert atmosphere

With pyridine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2014.02.023

Reference yield:

: 1595121-87-1
2-(trimethylsilyl)ethyl 6-O-acetyl-2,3-di-O-(p-methoxybenzyl)-β-D-glucopyranoside

: 1595122-13-6
2-(trimethylsilyl)ethyl (4-O-acetyl-2,3-di-O-benzoyl-6-deoxy-6-methylseleno-β-D-galactopyranosyl)-(1→4)-6-O-acetyl-2,3-di-O-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 3 h / -40 °C / Inert atmosphere; Molecular sieve

2.1: trifluoroacetic acid / dichloromethane / 2.5 h / -20 °C / Inert atmosphere

3.1: pyridine / 24 h / 20 °C / Cooling with ice; Inert atmosphere

With pyridine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2014.02.023