N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine

Base Information

Chemical Name:N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine
CAS No.:1379538-75-6
Molecular Formula:C₂₁H₂₉NO₂
Molecular Weight:327.467
Hs Code.:

Synonyms:N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine

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Chemical Property of N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine

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Technology Process of N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine

There total 1 articles about N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1085526-67-5
(4-tert-butylphenyl)ethynyl bromide

: 91230-06-7
3--2-methylprop-1-ene

: 1379538-75-6
N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine

Guidance literature:: With potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; In toluene; for 48h; Inert atmosphere; Reflux;
DOI:10.1021/ja303002a

Reference yield: 100.0%

: 1379538-75-6
N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine

: 1379538-57-4
N-tert-butoxycarbonyl-3-(4-tert-butylphenyl)-5-methyl-1,4-dihydropyridine

Guidance literature:: N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 1h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.1021/ja303002a

Reference yield: 88.0%

: 1379538-75-6
N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine

: 1379538-62-1
3-(4-tert-butylphenyl)-5-methylpyridine

Guidance literature:: N-(2-methylallyl)-N-tert-butoxycarbonyl-(4-tert-butylphenyl)ethynylamine; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 1h; Inert atmosphere;

With o-tetrachloroquinone; acetic acid; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.1021/ja303002a