S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate

Base Information

• Chemical Name: S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate
• CAS No.: 1243579-30-7
• Molecular Formula: C₂₁H₁₈BrNO₄S₂
• Molecular Weight: 492.414
• Mol file: 1243579-30-7.mol

Synonyms:S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate

Chemical Property of S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate

There total 1 articles about S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

N-vinylphthalimide (3485-84-5,26809-43-8) + dithiocarbonic acid S-[2-(4-bromo-phenyl)-2-oxo-ethyl] ester O-ethyl ester (1861-48-9) → S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate (1243579-30-7)

Guidance literature:

N-vinylphthalimide; dithiocarbonic acid S-[2-(4-bromo-phenyl)-2-oxo-ethyl] ester O-ethyl ester; In 1,2-dichloro-ethane; Inert atmosphere; Reflux;

With dilauryl peroxide; In 1,2-dichloro-ethane; Inert atmosphere;

DOI:10.1016/j.tet.2010.05.107

Reference yield:

(2-propenyl)propanedioic acid diethyl ester (2049-80-1) + S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate (1243579-30-7) → C31H34BrNO8S2

Guidance literature:

(2-propenyl)propanedioic acid diethyl ester; S-[4-(4-bromo-phenyl)-1-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-oxo-butyl]-O-ethyl dithiocarbonate; In 1,2-dichloro-ethane; for 0.25h; Inert atmosphere; Reflux;

With dilauryl peroxide; In 1,2-dichloro-ethane; Inert atmosphere;

DOI:10.1016/j.tet.2010.05.107

upstream raw materials:

N-vinylphthalimide

dithiocarbonic acid S-[2-(4-bromo-phenyl)-2-oxo-ethyl] ester O-ethyl ester