Technology Process of (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(II) bis-(2,6-xylyl)isocyanide
There total 1 articles about (7,8-dihydro-5,10,15,20-tetraphenylporphyrin) iron(II) bis-(2,6-xylyl)isocyanide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Zn-Hg;
In
dichloromethane;
under Ar; reduction of Fe(III) complex with Zn-Hg amalgam at room temp. for 1 h; 8 equiv. of isocyanide added; stirring for 12 h; filtered; hexane added gradually; after standing for 3 d, crystals collected; elem. anal.;
DOI:10.1039/b100925g