perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate

Base Information

Chemical Name:perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate
CAS No.:905575-65-7
Molecular Formula:C₃₀H₄₁F₅N₄O₈S
Molecular Weight:712.736
Hs Code.:

Synonyms:perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate

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Chemical Property of perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate

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Technology Process of perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate

There total 5 articles about perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 318511-05-6
4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oic acid

: 142685-25-4
2,3,5,6-tetrafluorophenyl 2,2,2-trifluoroacetate

: 905575-65-7
perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 0.5h;
DOI:10.1039/c0ob00060d

Reference yield: 54.0%

: 14533-84-7
pentafluorophenyl trifloroacetate

: 318511-05-6
4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oic acid

: 905575-65-7
perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/acs.jmedchem.9b00455

Reference yield:

: 4246-51-9
4,7,10-trioxa-1,13-diaminotridecane

: 905575-65-7
perfluorophenyl 4,20-dioxo-24-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-9,12,15-trioxa-5,19-diazatetracosan-1-oate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2.5 h / 0 - 20 °C / Inert atmosphere

With triethylamine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1021/acs.jmedchem.9b00455