methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

Base Information

Chemical Name:methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate
CAS No.:484046-55-1
Molecular Formula:C₃₅H₆₂O₁₇
Molecular Weight:754.867
Hs Code.:

Synonyms:methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

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Chemical Property of methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

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Technology Process of methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

There total 4 articles about methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 99-24-1
methyl galloate

: 62921-76-0,58320-73-3
2,5,8,11-tetraoxatridecan-13-ol tosylate

: 484046-55-1
methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; at 80 ℃; for 8h; Inert atmosphere;
DOI:10.1002/chem.201404941

Reference yield: 67.8%

: 99-24-1
methyl galloate

: 57722-04-0
1-chloro-2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethane

: 484046-55-1
methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

Guidance literature:: With potassium hydrogencarbonate; potassium iodide; In acetone; for 72h; Heating;

Reference yield:

: 23783-42-8,95507-80-5
tetraethylene glycol monomethyl ether

: 484046-55-1
methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / SOCl₂; pyridine

2: 67.8 percent / KHCO₃; KI / acetone / 72 h / Heating

With pyridine; thionyl chloride; potassium hydrogencarbonate; potassium iodide; In acetone;