5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid

Base Information

Chemical Name:5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid
CAS No.:1621060-25-0
Molecular Formula:C₂₀H₁₁ClF₄N₂O₄
Molecular Weight:454.765
Hs Code.:

Synonyms:5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid

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Chemical Property of 5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid

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Technology Process of 5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid

There total 5 articles about 5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₁₅ClF₄N₂O₄

: 1621060-25-0
5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid

Guidance literature:: With sodium hydride; at 100 ℃; for 0.166667h;

Reference yield:

: 1996-41-4
2-chloro-4-fluorophenol

: 1621060-25-0
5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 100 °C

2: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / acetonitrile; water; tert-butyl alcohol / 1 h / 0 - 25 °C

3: HATU; 4-methyl-morpholine / 8 h / 100 °C

4: sodium hydride / 0.17 h / 100 °C

With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydride; caesium carbonate; HATU; In water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

Reference yield:

: 1621060-65-8
2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzaldehyde

: 1621060-25-0
5-(2-(2-chloro-4-fluorophenoxy)-6-(trifluoromethyl)benzamido)picolinic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / acetonitrile; water; tert-butyl alcohol / 1 h / 0 - 25 °C

2: HATU; 4-methyl-morpholine / 8 h / 100 °C

3: sodium hydride / 0.17 h / 100 °C

With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium hydride; HATU; In water; acetonitrile; tert-butyl alcohol;