N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide

Base Information

Chemical Name:N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide
CAS No.:1192928-19-0
Molecular Formula:C₂₄H₂₂ClN₃O₆
Molecular Weight:483.908
Hs Code.:

Synonyms:N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide

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Chemical Property of N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide

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Technology Process of N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide

There total 5 articles about N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1192927-83-5
3,4,5-trimethoxy-N-((3-(4-chlorobenzoyl)aminophenylamino)carbonothioyl)benzamide

: 1192928-19-0
N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide

Guidance literature:: With copper(l) chloride; sodium hydroxide; In acetonitrile; at 120 ℃; for 0.1h; under 2585.81 Torr; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jm2013369

Reference yield:

: 118-41-2
Eudesmic acid

: 1192928-19-0
N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride

2: acetone / 0.33 h / Inert atmosphere; Reflux

3: acetone / 1 h / Inert atmosphere; Reflux

4: copper(l) chloride; sodium hydroxide / acetonitrile / 0.1 h / 120 °C / 2585.81 Torr / Inert atmosphere; Microwave irradiation

With oxalyl dichloride; copper(l) chloride; sodium hydroxide; In acetone; acetonitrile;
DOI:10.1021/jm2013369

Reference yield:

: 6282-15-1
4-chloro-benzoic acid-(3-nitro-anilide)

: 1192928-19-0
N-(3-(4-chlorobenzoylamino-2-methylphenyl-amino)carbonyl)-3,4,5-trimethoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; tin(II) chloride hydrate / ethanol / 60 °C / Inert atmosphere

2: acetone / 1 h / Inert atmosphere; Reflux

3: copper(l) chloride; sodium hydroxide / acetonitrile / 0.1 h / 120 °C / 2585.81 Torr / Inert atmosphere; Microwave irradiation

With hydrogenchloride; tin(II) chloride hydrate; copper(l) chloride; sodium hydroxide; In ethanol; acetone; acetonitrile;
DOI:10.1021/jm2013369