dibutyl γ-phenylallylphosphonate

Base Information

• Chemical Name: dibutyl γ-phenylallylphosphonate
• CAS No.: 145728-73-0
• Molecular Formula: C₁₇H₂₇O₃P
• Molecular Weight: 310.373
• Mol file: 145728-73-0.mol

Synonyms:dibutyl γ-phenylallylphosphonate

Chemical Property of dibutyl γ-phenylallylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of dibutyl γ-phenylallylphosphonate

There total 2 articles about dibutyl γ-phenylallylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

dibutyl hydrogen phosphite (1809-19-4) + 1-phenyl-2-propenyl acetate (7217-71-2) → dibutyl γ-phenylallylphosphonate (145728-73-0)

Guidance literature:

With BAS; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; In tetrahydrofuran; for 15h; Heating;

DOI:10.1055/s-1986-31704

Reference yield: 79.0%

iodobenzene (591-50-4) + allyl phophonate de dibutyl (4762-64-5) → dibutyl γ-phenylallylphosphonate (145728-73-0)

Guidance literature:

With palladium diacetate; triethylamine; triphenylphosphine; at 100 ℃; for 18h;

DOI:10.1007/BF00869543

upstream raw materials:

dibutyl hydrogen phosphite

1-phenyl-2-propenyl acetate

iodobenzene

allyl phophonate de dibutyl