4,10-bis(p-tolylsulphonyl)-7,16,19,24,27-pentaoxa-1,4,10,13-tetra-azabicyclo<11.8.8>nonacosane

Base Information

Chemical Name:4,10-bis(p-tolylsulphonyl)-7,16,19,24,27-pentaoxa-1,4,10,13-tetra-azabicyclo<11.8.8>nonacosane
CAS No.:111306-32-2
Molecular Formula:C₃₄H₅₄N₄O₉S₂
Molecular Weight:726.956
Hs Code.:

Synonyms:4,10-bis(p-tolylsulphonyl)-7,16,19,24,27-pentaoxa-1,4,10,13-tetra-azabicyclo<11.8.8>nonacosane

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Chemical Property of 4,10-bis(p-tolylsulphonyl)-7,16,19,24,27-pentaoxa-1,4,10,13-tetra-azabicyclo<11.8.8>nonacosane

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Technology Process of 4,10-bis(p-tolylsulphonyl)-7,16,19,24,27-pentaoxa-1,4,10,13-tetra-azabicyclo<11.8.8>nonacosane

There total 3 articles about 4,10-bis(p-tolylsulphonyl)-7,16,19,24,27-pentaoxa-1,4,10,13-tetra-azabicyclo<11.8.8>nonacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 5414-19-7
1,1'-oxybis(2-bromo-ethane)

: 76343-82-3
7,16-bis<2-(p-tolylsulphonylamino)ethyl>-1,4,10-tetraoxa-7,16-diazacyclo-octadecane

: 111306-32-2
4,10-bis(p-tolylsulphonyl)-7,16,19,24,27-pentaoxa-1,4,10,13-tetra-azabicyclo<11.8.8>nonacosane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In toluene; for 16h; Heating;

Reference yield:

: 3634-89-7
N-(p-toluenesulfonyl)aziridine

: 111306-32-2
4,10-bis(p-tolylsulphonyl)-7,16,19,24,27-pentaoxa-1,4,10,13-tetra-azabicyclo<11.8.8>nonacosane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / acetonitrile / Heating

2: 1.) C₂H₅ONa / 2.) DMF, 100 deg C, 16 h

With sodium ethanolate; In acetonitrile;