N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide

Base Information

Chemical Name:N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide
CAS No.:1296210-51-9
Molecular Formula:C₂₂H₁₉N₅O₇S
Molecular Weight:497.488
Hs Code.:

Synonyms:N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide

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Chemical Property of N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide

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Technology Process of N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide

There total 4 articles about N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₆ClN₃O₃S

: 3291-03-0
3,4,5-trimethoxybenzohydrazide

: 1296210-51-9
N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 36.5h;
DOI:10.1016/j.bmc.2011.01.050

Reference yield:

: 4521-33-9
5-nitro-2-thiophenecarboxaldehyde

: 1296210-51-9
N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: nitrobenzene / 8 h / Reflux

2: thionyl chloride / benzene / 12 h / Reflux

3: dmap / dichloromethane / 36.5 h / 0 - 20 °C

With dmap; thionyl chloride; In dichloromethane; nitrobenzene; benzene;
DOI:10.1016/j.bmc.2011.01.050

Reference yield:

: 2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carboxylic acid

: 1296210-51-9
N'-(3,4,5-trimethoxybenzoyl)-2-(5-nitrothiophen-2-yl)-1H-benzo[d]imidazole-5-carbohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / benzene / 12 h / Reflux

2: dmap / dichloromethane / 36.5 h / 0 - 20 °C

With dmap; thionyl chloride; In dichloromethane; benzene;
DOI:10.1016/j.bmc.2011.01.050