N¹,N³,N⁵-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide

Base Information

• Chemical Name: N¹,N³,N⁵-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide
• CAS No.: 1424097-99-3
• Molecular Formula: C₉₀H₁₄₇N₃O₁₈
• Molecular Weight: 1559.17

Synonyms:N¹,N³,N⁵-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide

Chemical Property of N¹,N³,N⁵-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide

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Technology Process of N¹,N³,N⁵-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide

There total 1 articles about N¹,N³,N⁵-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.4%

1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-amine (1424097-97-1) + 1,3,5-benzene tris(carbonyl chloride) (4422-95-1) → N1,N3,N5-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide (1424097-99-3)

Guidance literature:

With triethylamine; In chloroform; at 0 - 20 ℃;

DOI:10.1039/c3cc38949a

Reference yield: 93.0%

N1,N3,N5-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide (1424097-99-3) → N1,N3,N5-tris(1-hydroxy-3,6,9,12-tetraoxatetracosan-24-yl)benzene-1,3,5-tricarboxamide (1424097-86-8)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃;

DOI:10.1039/c3cc38949a

Reference yield: 53.0%

N1,N3,N5-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide (1424097-99-3) + methyl iodide (74-88-4) → N1,N3,N5-trimethyl-N1,N3,N5-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide (1424098-01-0)

Guidance literature:

N¹,N³,N⁵-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; mineral oil; for 16h; Reflux;

DOI:10.1039/c3cc38949a

upstream raw materials:

1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-amine

1,3,5-benzene tris(carbonyl chloride)

Downstream raw materials:

N¹,N³,N⁵-tris(1-hydroxy-3,6,9,12-tetraoxatetracosan-24-yl)benzene-1,3,5-tricarboxamide

N¹,N³,N⁵-trimethyl-N¹,N³,N⁵-tris(1-phenyl-2,5,8,11,14-pentaoxahexacosan-26-yl)benzene-1,3,5-tricarboxamide

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