5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

Base Information

Chemical Name:5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone
CAS No.:1353346-40-3
Molecular Formula:C₅₄H₃₈Cl₄N₁₈O₄
Molecular Weight:1144.83
Hs Code.:

5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

Synonyms:5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

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Chemical Property of 5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

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Technology Process of 5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

There total 3 articles about 5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1254568-80-3
6-(4-ethynylbenzyl)-1,3,5-triazine-2,4-diamine

: 1353346-36-7
N,N'-bis(3-azidopropyl)-1,6,7,12-tetrachloroperylene-3,4:9,10-bis(dicarboximide)

: 1353346-40-3
5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; isopropyl alcohol; toluene; at 90 ℃; for 7h; cavity resonator;
DOI:10.1016/j.tet.2011.10.096

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1353346-40-3
5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1: chlorosulfonic acid; iodine / 5 h / 70 °C

2: toluene / 4 h / Inert atmosphere; Reflux

3: copper(l) iodide; N-ethyl-N,N-diisopropylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; isopropyl alcohol; toluene / 7 h / 90 °C / cavity resonator

With chlorosulfonic acid; copper(l) iodide; iodine; N-ethyl-N,N-diisopropylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; isopropyl alcohol; toluene;
DOI:10.1016/j.tet.2011.10.096

Reference yield:

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

: 1353346-40-3
5,6,12,13-tetrachloro-2,9-bis(3-(4-(4-((4,6-diamino-1,3,5-triazin-2-yl)methyl)phenyl)-1H-1,2,3-triazol-1-yl)propyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 4 h / Inert atmosphere; Reflux

2: copper(l) iodide; N-ethyl-N,N-diisopropylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; isopropyl alcohol; toluene / 7 h / 90 °C / cavity resonator

With copper(l) iodide; N-ethyl-N,N-diisopropylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; isopropyl alcohol; toluene;
DOI:10.1016/j.tet.2011.10.096