C₄₂H₆₀O₉SSi

Base Information

• Chemical Name: C₄₂H₆₀O₉SSi
• CAS No.: 1380204-54-5
• Molecular Formula: C₄₂H₆₀O₉SSi
• Molecular Weight: 769.085
• Mol file: 1380204-54-5.mol

Synonyms:C₄₂H₆₀O₉SSi

Chemical Property of C₄₂H₆₀O₉SSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₂H₆₀O₉SSi

There total 6 articles about C₄₂H₆₀O₉SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C41H58O7Si (1380204-51-2) + methanesulfonyl chloride (124-63-0) → C42H60O9SSi (1380204-54-5)

Guidance literature:

With N,N,N'N'-tetramethyl-1,3-propanediamine; In toluene; at 0 - 20 ℃; for 1h;

DOI:10.1002/anie.201201383

Reference yield:

C12H14O3 → C42H60O9SSi (1380204-54-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

1.2: 2 h / -78 °C

2.1: Hoveyda-Grubbs catalyst second generation / toluene / Reflux

3.1: N,N,N'N'-tetramethyl-1,3-propanediamine / toluene / 1 h / 0 - 20 °C

With Hoveyda-Grubbs catalyst second generation; N,N,N'N'-tetramethyl-1,3-propanediamine; sodium hexamethyldisilazane; In tetrahydrofuran; toluene;

DOI:10.1002/anie.201201383

Reference yield:

C31H48O4Si → C42H60O9SSi (1380204-54-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

1.2: 2 h / -78 °C

2.1: Hoveyda-Grubbs catalyst second generation / toluene / Reflux

3.1: N,N,N'N'-tetramethyl-1,3-propanediamine / toluene / 1 h / 0 - 20 °C

With Hoveyda-Grubbs catalyst second generation; N,N,N'N'-tetramethyl-1,3-propanediamine; sodium hexamethyldisilazane; In tetrahydrofuran; toluene;

DOI:10.1002/anie.201201383

upstream raw materials:

C₄₃H₆₀O₇Si

C₄₁H₅₆O₇Si

C₄₁H₅₈O₇Si

methanesulfonyl chloride

Downstream raw materials:

C₃₁H₄₆O₄SeSi

C₃₇H₆₀O₄SeSi₂

C₃₇H₅₈O₄SeSi₂

C₄₀H₆₆O₄SeSi₃