β-phenylethyl trichloroacetimidate

Base Information

Chemical Name:β-phenylethyl trichloroacetimidate
CAS No.:99421-73-5
Molecular Formula:C₁₀H₁₀Cl₃NO
Molecular Weight:266.554
Hs Code.:

Synonyms:β-phenylethyl trichloroacetimidate

Suppliers and Price of β-phenylethyl trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-phenylethyl trichloroacetimidate

Chemical Property:

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Technology Process of β-phenylethyl trichloroacetimidate

There total 1 articles about β-phenylethyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 60-12-8
2-phenylethanol

: 545-06-2
trichloroacetonitrile

: 99421-73-5
β-phenylethyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1021/jacs.7b05214

Reference yield: 99.0%

: 99421-73-5
β-phenylethyl trichloroacetimidate

: 4-phenyl-2-(trichloromethyl)-4,5-dihydrooxazole

Guidance literature:: With iodine; (2-(N-methylbenzamido)phenyl)-l 3-iodanediyl diacetate; potassium carbonate; In dichloromethane; at 20 ℃; for 3h; Irradiation;
DOI:10.1002/adsc.202100316

Reference yield: 91.0%

: 99421-73-5
β-phenylethyl trichloroacetimidate

: 20989-17-7,56613-80-0,71006-16-1,7568-92-5,188586-38-1
Phenylglycinol

Guidance literature:: β-phenylethyl trichloroacetimidate; With phthaloyl peroxide; cesium iodide; In acetonitrile; at 20 ℃; for 2h; Irradiation; Inert atmosphere;

With hydrogenchloride; In methanol; water; acetonitrile; for 2h; Reagent/catalyst; Inert atmosphere;
DOI:10.1002/anie.202008806