1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone

Base Information

Chemical Name:1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone
CAS No.:82323-19-1
Molecular Formula:C₂₉H₃₂N₂O₂S
Molecular Weight:472.651
Hs Code.:

Synonyms:1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone

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Chemical Property of 1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone

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Technology Process of 1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone

There total 7 articles about 1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.6%

: 82323-52-2
1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 82323-19-1
1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone

Guidance literature:: With hydrogenchloride; In ethanol; at 40 ℃; for 0.0833333h;
DOI:10.1021/jo00139a002

Reference yield:

: 18932-33-7
4-methyl-4-phenylcyclohexan-1-one

: 82323-19-1
1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) n-butyllithium / 1.) THF, hexane, 0 deg C, 15 min, 2.) from 0 deg C to reflux, 3 h

2: 99.5 percent / Br₂ / diethyl ether / 0.5 h / Heating

3: 95.1 percent / KOH / ethanol / 0.25 h / 50 °C

4: 1.) Mg (powder) / 1.) THF, reflux, 2 h

5: 91.6 percent / diethyl ether / 3 h / 22 °C

6: 75.6 percent / HCl / ethanol / 0.08 h / 40 °C

With hydrogenchloride; potassium hydroxide; n-butyllithium; bromine; magnesium; In diethyl ether; ethanol;
DOI:10.1021/jo00139a002

Reference yield:

: 1100-88-5
benzyltriphenylphosphonium chloride

: 82323-19-1
1-(4-methyl-4-phenylcyclohexylidene)-1-phenyl-2-propanone tosylhydrazone

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) n-butyllithium / 1.) THF, hexane, 0 deg C, 15 min, 2.) from 0 deg C to reflux, 3 h

2: 99.5 percent / Br₂ / diethyl ether / 0.5 h / Heating

3: 95.1 percent / KOH / ethanol / 0.25 h / 50 °C

4: 1.) Mg (powder) / 1.) THF, reflux, 2 h

5: 91.6 percent / diethyl ether / 3 h / 22 °C

6: 75.6 percent / HCl / ethanol / 0.08 h / 40 °C

With hydrogenchloride; potassium hydroxide; n-butyllithium; bromine; magnesium; In diethyl ether; ethanol;
DOI:10.1021/jo00139a002